1-N-Boc-2-Methylhydrazine synthesis
- Product Name:1-N-Boc-2-Methylhydrazine
- CAS Number:127799-54-6
- Molecular formula:C6H14N2O2
- Molecular Weight:146.19
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: 64 percent / toluene / 6 h
2.1: n-BuLi / tetrahydrofuran; hexane / 1 h / cooling
2.2: tetrahydrofuran; hexane / 5 h
2.3: 83 percent / aq. NaOH / CH2Cl2 / 0.5 h / 20 °C
References:
Melendez, Rosa E.;Lubell, William D. [Journal of the American Chemical Society,2004,vol. 126,# 21,p. 6759 - 6764]
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