1-Hydroxycyclopentanecarboxylic acid. synthesis
- Product Name:1-Hydroxycyclopentanecarboxylic acid.
- CAS Number:16841-19-3
- Molecular formula:C6H10O3
- Molecular Weight:130.14
25438-35-1
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16841-19-3
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Yield:16841-19-3 94%
Reaction Conditions:
with hydrogenchloride in acetic acid at 80; for 4 h;
Steps:
8
8a (3 g, 16.36 mmol 1 .00 equiv) was dissolved in acetic acid (4 mL) and concentrated hydrogen chloride (4 mL). The resulting solution was stirred for 4 h at 80 °C. The mixture was then concentrated under reduced pressure to give 8b (2 g, 94%) as a white solid, which was used without further purification.
References:
WO2013/96771,2013,A1 Location in patent:Page/Page column 100
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16841-19-3
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16841-19-3
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16841-19-3
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