1-chloro-4-dichlorophosphorylbenzene synthesis
- Product Name:1-chloro-4-dichlorophosphorylbenzene
- CAS Number:22585-81-5
- Molecular formula:C6H4Cl3OP
- Molecular Weight:229.43
Yield:22585-81-5 92%
Steps:
9 EXAMPLE 9
EXAMPLE 9 90 g of p-chlorophenylphosphonic acid dimethyl ester were heated in the apparatus described in Example 1 at 110°C. At this temperature phosgene was introduced for 5.5 hours and subsequently the reaction mixture was distilled. 86 g of p-chlorophenylphosphonic acid dichloride were obtained, b.p. 91°-93°C.0.2 mm Hg corresponding to a yield of 92 percent of the theory.
References:
US3950413,1976,A
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