1-(4-Methylphenyl)ethanol synthesis
- Product Name:1-(4-Methylphenyl)ethanol
- CAS Number:536-50-5
- Molecular formula:C9H12O
- Molecular Weight:136.19
622-96-8
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536-50-5
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Yield:536-50-5 93%
Reaction Conditions:
with C22H30B10Cl2FeN6O2;dihydrogen peroxide in methanol at 20; for 7 h;
Steps:
10
4-methylethylbenzene (1.0 mmol), iron complex 2 (0.05 mmol) and H2O2 (1.3 mmol) were dissolved in 2 mL of methanol and reacted at room temperature for 7 hours. After the reaction was completed, the reaction solution was concentrated and separated directly by silica gel column chromatography. Drying to the same mass yields the corresponding product C9H12O (93% yield).
References:
CN110627841,2019,A Location in patent:Paragraph 0069-0072
122-00-9
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536-50-5
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$29.00/1g
622-97-9
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$10.00/5mL
536-50-5
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$29.00/1g
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536-50-5
109 suppliers
$29.00/1g