1,2-BIS(TRICHLOROSILYL)ETHANE synthesis
- Product Name:1,2-BIS(TRICHLOROSILYL)ETHANE
- CAS Number:2504-64-5
- Molecular formula:C2H4Cl6Si2
- Molecular Weight:296.94
107-06-2
436 suppliers
$14.00/25g
2504-64-5
88 suppliers
$29.00/5g
Yield: 65.4%
Reaction Conditions:
with trichlorosilane;tetra-n-butylphosphonium chloride at 150; for 6 h;Autoclave;
Steps:
10 The reaction of the 1,2-dichloroethane and trichlorosilane (Catalyst: tetrabutylphosphonium chloride)
3.8 g (13mmol) tetrabutylphosphonium chloride and 12.6 g(0.13mol) of 1,2- dichloroethane and 88 g (0.65mol) of the trichlorosilane wasreacted in the stainless steel high pressure reactor with 120 milliliters for 6 hours at 150°C and the 1,2-bis(trichlorosilyl) ethane of 25.2 g (yield 65.4%)was obtained in the same manner as that of above described embodiment 4.
References:
JSI SILICONE Co., Ltd;JUNG, IR NAM;KIM, UHN SUNG;KIM, SUNG MIN;KIM, YOUNG MIN KR2015/101288, 2015, A Location in patent:Paragraph 0071; 0072
75-94-5
212 suppliers
$20.00/25g
2504-64-5
88 suppliers
$29.00/5g
75-94-5
212 suppliers
$20.00/25g
10025-78-2
186 suppliers
$22.50/25g
2504-64-5
88 suppliers
$29.00/5g
5283-66-9
124 suppliers
$12.00/5 g
107-06-2
436 suppliers
$14.00/25g
2504-64-5
88 suppliers
$29.00/5g