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[ CAS No. 4815-30-9 ] {[proInfo.proName]}

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Chemical Structure| 4815-30-9
Chemical Structure| 4815-30-9
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Product Details of [ 4815-30-9 ]

CAS No. :4815-30-9 MDL No. :MFCD00005450
Formula : C11H15NO4S Boiling Point : No data available
Linear Structure Formula :CH3CO2C2H5C7H7O2NS InChI Key :DGVXLHAJVRRLGV-UHFFFAOYSA-N
M.W : 257.31 Pubchem ID :78537
Synonyms :

Safety of [ 4815-30-9 ]

Signal Word:Warning Class:
Precautionary Statements:P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313 UN#:
Hazard Statements:H315-H319 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 4815-30-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 4815-30-9 ]

[ 4815-30-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 13781-53-8 ]
  • [ 4815-30-9 ]
  • [ 917087-61-7 ]
YieldReaction ConditionsOperation in experiment
Production Example 1 Ethyl 5-methyl-4-oxo-2-(thiophen-3-ylmethyl)-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxylate 515 Milligrams of diethyl 5-amino-3-methylthiophene-2,4-dicarboxylate and 296 mg of 3-thiopheneacetonitrile were added to 8 mL of 4N hydrogen chloride-dioxane solution and stirred for 10 hours. Thereafter the liquid reaction mixture was poured on ice, and its pH was adjusted to 8 - 9 with 25% aqueous ammonia. Whereupon precipitated crystals were recovered by filtration and washed first with water, and then with hexane. The crude crystals were recrystallized from a liquid mixture of N,N-dimethylformamide and cyclohexane, to provide 397 mg of the title compound. 1H-NMR(DMSO-d6) δ: 1.30(3H,t,J=7, 1Hz),2.81(3H,s), 3.97(2H,s),4.30(2H,q,J=7.1Hz),7.0-7.6(3H,m),12.74(1H,br s) MS(m/z):334(M+)
With hydrogenchloride; In 1,4-dioxane; cyclohexane; N,N-dimethyl-formamide; 1-a : Synthesis of ethyl 5-methyl-4-oxo-2-(thiophen-3-ylmethyl)-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxylate To 8 mL of 4N hydrogen chloride in dioxane solution, 515 mg of diethyl 5-amino-3-methylthiophene-2,4-dicarboxylate and 296 mg of 3-thiopheneacetonitrile were added, and stirred for 10 hours. Thereafter the liquid reaction mixture was poured on ice, and its pH was adjusted to 8-9 with 25% aqueous ammonia. Whereupon precipitated crystals were recovered by filtration and washed with water and hexane, by the order stated. The crude crystals were recrystallized from a liquid mixture of N,N-dimethylformamide and cyclohexane, to provide 397 mg of the title compound. 1H-NMR(DMSO-d6)δ:1.30(3H,t,J=7.1Hz),2.81(3H,s),3.97(2H,s), 4.30(2H,q,J=7.1Hz),7.0-7.6(3H,m),12.74(1H,br s) MS(m/z):334(M+)
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