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[ CAS No. 3114-61-2 ] {[proInfo.proName]}

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Chemical Structure| 3114-61-2
Chemical Structure| 3114-61-2
Structure of 3114-61-2 * Storage: {[proInfo.prStorage]}

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Product Details of [ 3114-61-2 ]

CAS No. :3114-61-2 MDL No. :MFCD16876801
Formula : C7H7NO4 Boiling Point : -
Linear Structure Formula :- InChI Key :URFJTCWCTWGRBB-UHFFFAOYSA-N
M.W : 169.13 Pubchem ID :15654643
Synonyms :

Safety of [ 3114-61-2 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P280-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 3114-61-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 3114-61-2 ]

[ 3114-61-2 ] Synthesis Path-Downstream   1~12

  • 1
  • [ 6665-97-0 ]
  • [ 3114-61-2 ]
  • 2
  • [ 6665-97-0 ]
  • [ 107-06-2 ]
  • [ 3114-61-2 ]
  • 3
  • [ 601-89-8 ]
  • [ 77-78-1 ]
  • [ 3114-61-2 ]
  • [ 6665-97-0 ]
  • 4
  • [ 3114-61-2 ]
  • [ 141815-91-0 ]
  • [ 1026658-72-9 ]
  • 5
  • [ 7446-70-0 ]
  • [ 6665-97-0 ]
  • [ 71-43-2 ]
  • [ 3114-61-2 ]
  • 6
  • [ 3114-61-2 ]
  • [ 91-66-7 ]
  • 4-methoxy-2-methylbenzo[d]oxazole [ No CAS ]
  • 7
  • [ 3114-61-2 ]
  • [ 149353-19-5 ]
  • 8
  • [ 3114-61-2 ]
  • N-[6-Methoxy-2-{3-(5-methyl-4-phenyl-1H-imidazol-1-yl) propoxy}]phenyl-N'-pentylurea [ No CAS ]
  • 9
  • [ 601-89-8 ]
  • [ 3114-61-2 ]
  • 10
  • [ 108-46-3 ]
  • [ 3114-61-2 ]
  • 11
  • [ 601-89-8 ]
  • [ 77-78-1 ]
  • [ 3114-61-2 ]
YieldReaction ConditionsOperation in experiment
37% With sodium hydroxide; In water; at 40℃; for 0.25h; Dimethylsulfate (2.7 mL, 0.058 mmol) was added carefully to 2-nitrobenzene-1,3-diol (2.5 g, 0.232 mmol) and the mixture was stirred vigorously while 10% NaOH solution (21 mL) was added and the temperature was kept below 40 C. After about 15 min, the mixture was cooled and then filtered. The filtrate was collected and acidified with 10% HCl, and extracted with ether (3×25 mL). The organic layer was dried (MgSO4), filtered, and concentrated under vacuum. Chromatography (10-30% EtOAc/hexanes) provided 9A10 (1 g, 37%).
  • 12
  • [ 3114-61-2 ]
  • 6-iodo-3-methoxy-2-nitro-phenol [ No CAS ]
YieldReaction ConditionsOperation in experiment
96% With iodine; sodium hydrogencarbonate; at 0 - 20℃; for 1.0h; Step 2: 6-Iodo-<strong>[3114-61-2]3-methoxy-2-nitrophenol</strong> A mixture of 1.36 g (8 mmol) of the product of Step 1 and 0.68 g (8 mmol) of sodium bicarbonate was sonicated at room temperature until it become homogenous. The resulting mixture was cooled to O0C and 2.04 g (8 mmol) of iodine was added. After stirring for 1 h at room temperature the precipitate formed was filtered off, dried and recrystallized from ethyl ether to give 2.28 g (96% yield of pure title compound as an orange crystals; 1H NMR (CDCl3) 3.92 (s, 3H, OMe); 6.41 (d, IH, CH J = 9Hz); 7.82 (d, IH5 J=9Hz); 10.37 (s, IH5 OH).
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