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ChemicalBook CAS DataBase List 1,4,6-Tri-O-acetyl-a-D-mannopyranose 2,3-Carbonate
53958-20-6

1,4,6-Tri-O-acetyl-a-D-mannopyranose 2,3-Carbonate synthesis

3synthesis methods
63167-67-9 Synthesis
Methyl 4,6-O-Isopropylidene-a-D-mannopyranoside

63167-67-9
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 74 percent / triethylamine / benzene; dioxane / 4 h / 0 °C
2: 1.) 90percent trifluoroacetic acid; 2.) sulphuric acid / 1.) ethanol, chloroform, 10 min, room t.; 2.) 4 h, room t.

References:

Betaneli, Vitali I.;Ovchinnikov, Michael V.;Backinowsky, Leon V.;Kochetkov, Nikolay K. [Carbohydrate Research,1980,vol. 84,p. 211 - 224]

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