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ChemicalBook CAS DataBase List Methyl 6-nitro-1H-indazole-3-carboxylate
1167056-71-4

Methyl 6-nitro-1H-indazole-3-carboxylate synthesis

3synthesis methods
70315-70-7 Synthesis
3-Iodo-6-nitroindazole

70315-70-7
197 suppliers
$10.00/250mg

201230-82-2 Synthesis
carbon monoxide

201230-82-2
1 suppliers
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Yield:1167056-71-4 38%

Reaction Conditions:

with 1,1'-bis-(diphenylphosphino)ferrocene;dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2;triethylamine in toluene at 70 - 80; under 750.075 Torr;Autoclave;

References:

Buchstaller, Hans-Peter;Wilkinson, Kai;Burek, Kasimir;Nisar, Yasmin [Synthesis,2011,# 19,art. no. T48411SS,p. 3089 - 3098] Location in patent:experimental part