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ChemicalBook CAS DataBase List TRIPHENYLACRYLONITRILE
6304-33-2

TRIPHENYLACRYLONITRILE synthesis

6synthesis methods
-

Yield:6304-33-2 81%

Reaction Conditions:

Stage #1: Triphenylvinyl bromidewith copper(I) oxide;oxygen;triphenylphosphine in 1-methyl-pyrrolidin-2-one;Schlenk technique;Sealed tube;
Stage #2: ethyl 2-cyanoacetatewith silver nitrate;acetic acid in 1-methyl-pyrrolidin-2-one at 130; for 18 h;Schlenk technique;Sealed tube;

References:

Wang, Xian-Jin;Zhang, Song-Lin [New Journal of Chemistry,2017,vol. 41,# 24,p. 14826 - 14830] Location in patent:supporting information

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